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Trainings from DRUCK & TEMPERATUR Leitenberger

Trainings
Briefings

SERVICES

Trainings of DRUCK & TEMPERATUR Leitenberger LR-Cal

From simple instructions to complex training courses on the topics of

  • Calibration of pressure gauges
    with working and primary standards
      
  • Calibration of temperature measuring instruments
    by means of comparative measurements with controlled temperature sources
      
  • Calibration of torque wrenches by means of precision torque measurement and clamping device for torque wrenches
      
  • Instruction in the commissioning and use of individual testing and calibration devices from our portfolio

From one participant to groups of up to about 25 people.
At our company in one of our training rooms.

Participants receive a certificate after successful completion.

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Read more …Trainings from DRUCK & TEMPERATUR Leitenberger

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Events

Events
Exhibitions

DRUCK & TEMPERATUR
Leitenberger GmbH
GERMANY

Fairs + Exhibitions

We will participate in the following trade fairs or exhibitions and look forward to meeting you there in person.


LR-Cal DRUCK & TEMPERATUR Leitenberger - GERMANY exhibits on CONTROL show 2027

CONTROL 2027

International trade fair for quality assurance

May 11-14, 2027 - Messe Stuttgart - GERMANY

Hall and booth numbers will be posted here shortly.

We cordially invite you to visit us at our stand. In addition to our new products, we will be presenting our portfolio of testing and calibration devices for pressure, temperature, level, torque and force.

Our team is looking forward to meeting you!


LR-Cal DRUCK & TEMPERATUR Leitenberger exhibits on the ACHEMA 2027 exhibition

ACHEMA 2027

World leading show for the process industry

June 14-18, 2027
Messe Frankfurt (Exhibition Center Frankfurt/Main)

Hall and booth numbers will be posted here shortly.

We cordially invite you to visit us at our stand.


  • DRUCK & TEMPERATUR Leitenberger (Germany) on trade fairs and exhibitions.
  • DRUCK & TEMPERATUR Leitenberger (Germany) on trade fairs and exhibitions.
  • DRUCK & TEMPERATUR Leitenberger (Germany) on trade fairs and exhibitions.
  • 2024 Achema 040

  • DRUCK & TEMPERATUR Leitenberger (Germany) on trade fairs and exhibitions.
  • DRUCK & TEMPERATUR Leitenberger (Germany) on trade fairs and exhibitions.
  • DRUCK & TEMPERATUR Leitenberger (Germany) on trade fairs and exhibitions.
  • DRUCK & TEMPERATUR Leitenberger (Germany) on trade fairs and exhibitions.
  • 2024 Achema 050

  • DRUCK & TEMPERATUR Leitenberger (Germany) on trade fairs and exhibitions.

Read more …Events

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Repairs

Repairs
Maintenances

SERVICES

Repairs + Maintenances

Even the best equipment and instruments need maintenance or even repair from time to time.

Repairs - a service of DRUCK & TEMPERATUR Leitenberger

Please send the device to be serviced or defective (make LR-Cal Leitenberger) cleaned, well packed and free to:

DRUCK & TEMPERATUR Leitenberger GmbH
Incoming goods SERVICE
Bahnhofstr. 33
72138 Kirchentellinsfurt
GERMANY

Upon receipt, our team will provide you with a confirmation of receipt and, after checking, a cost estimate for your approval.

However, please note:
We protect our employees in incoming goods and repair. Please make sure that sent in devices are free of hazardous substances, cleaned as well as well packed.

Please fill out the following return form for each device sent in and enclose it with your shipment.

Please fill out this return form for each device to be sent in and enclose it with the shipment.

Return form

Read more …Repairs

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LR-Cal BK 40-M temperature calibration bath

LR-Cal BK 40-M
Stationary temperature calibration bath
-40...+125°C

LR-Cal BK 40-M stationary temperature calibration bath LR-Cal
  • Stationary
  • Temperature range -40°C...+125°C
  • Accuracy ±0.2°C, stability ±0.05°C
  • Calibration bath made of stainless steel, useful diameter 85 mm, depth 340 mm
  • Option: Version -2I with 2 measuring inputs for Pt 100 or thermocouples
  • Option: Vertical overflow system for even higher temperature uniformity
  • control panel of the LR-Cal BK 40-M calibration bath

    Bedienpanel

    LR-Cal BK 40-M
    control panel

  • Optional vertical overflow system of the calibration bath LR-Cal BK 40-M

    Überströmsystem

    optional vertical
    overflow system

  • Scheme of the optional vertical overflow system LR-Cal BK 40-M

    Scheme: overflow syste

    Scheme of the
    optional vertical
    overflow system

  • Description

    LR-Cal BK 40-M description

    The portable temperature calibration bath LR-Cal BK 40-M serves as a temperature source and reference instrument in one, for testing and calibrating temperature measuring instruments of all kinds. It is particularly suitable for laboratory and glass thermometers.

    It features a particularly robust design, with stainless steel liquid container, and modern microprocessor control.

    The large usable volume of approx. 10 liters ensures high temperature stability over the entire range, thus simultaneous calibration of several test items is possible without any problems. The vessel is filled with a suitable calibration medium, which is constantly kept in a homogeneous state by means of a vertical stirrer. The stirrer is driven by an 80W electric motor. The equipment is also equipped with a safety temperature limiter, an overflow and a valve for emptying the heating tank.

    Optionally, the LR-Cal BK 40-M temperature calibration bath can be equipped with a vertical overflow system to further improve temperature stability and uniformity.

    The thermostatic temperature calibration bath LR-Cal BK 40-M is used

    • Testing and calibration of temperature sensors
    • Testing and calibration of glass thermometers
    • Testing and calibration of measuring temperature chains
    • Testing and adjustment of thermostats and thermostatic valves
  • Variants/designs

    LR-Cal BK 40-M Variants/designs

    Code Variant / design
    BK40-M Normal standard version
    BK40-M-TR Variant with vertical overflow system for further improvement of temperature uniformity
    BK40-M-2I Version -2I with two measuring inputs for Pt 100 / thermocouples *)
    BK40-M-TR-2I Version with vertical overflow system and with two measuring inputs for Pt 100 / thermocouples *)

     

    *) Accuracy (maximum deviation) of the two measuring inputs for device version "-2I":
    Pt 100 or Pt 1000 at -40°C: ±0.09°C at 0°C: ±0.08°C at +150°C: ±0.11°C at +300°C: ±0,14°C
    Thermocouple type B at +950°C: ±0.97°C at +1,050°C: ±1.03°C at +1,200°C: ±1.12°C    
    Thermocouple type E at -40°C: ±0.42°C at 0°C: ±0.40°C at +350°C: ±0.61°C    
    Thermocouple type J at +200°C: ±0.52°C at +450°C: ±0.67°C at +700°C: ±0.82°C    
    Thermocouples types K, N, R and S at +400°C: ±0.64°C at +700°C: ±0.82°C at +1,000°C: ±1.00°C    
    Thermocouple type T at -40°C: ±0.42°C at 0°C: ±0.40°C at +350°C: ±0.61°C    
  • Specification

    LR-Cal BK 40-M specification

    Description: Data:
    Temperature range -40°C...+125°C
    Stability ±0.05°C
    Uniformity 0.02°C radial and axial
    Stability indication audiovisual
    Accuracy ±0.2°C at +120°C
    Display resolution 0.01°C
    Temperature indication °C / °F switchable
    Interface RS232
    Thermostat test circuit 12V
    Ramp function yes
    Switch test yes
    Bath containter Stainless steel, usable diamter 85 mm, depth 340 mm
    Versorgung 230 VAC ±10% (optional, on request: 115 VAC)
    Leistungsaufnahme 2500 W
    Gewicht approx. 60 kg (Shipping weight approx. 74 kg)
    Abmessung 450 x 450 x 925 / 1300 mm
  • Scope of standard supply

    LR-Cal BK 40-M scope of standard supply

    • Stationary temperature calibration bath LR-Cal BK 40-M
    • Tank cover with 5 holes, 16 mm diameter, with guide tube
    • Spare fuses
    • Cable for power supply
    • Connection cables for thermostat tests
    • Holding device for test specimens
    • only for -2I versions: Connection cable red/black, screw terminals red/black, for both measuring inputs
    • Factory certificate of calibration
    • Operating manual EN
  • Calibration liquids + Accessories

LR-Cal BK 40-M calibration liquids + accessories

  • Calibration liquid
    Glycol

    Code: GLYCOL

    Can with 10 kg
    Ethylenic glycol 56%
    Application range -40...+80°C
    Smoke flash point at 110°C
    A viscosity of 10 cst
    exists at +20°C
    Freezing temperature -43°C

    For units with vertical overflow system to be used for temperatures -40...+1°C.

    For devices without vertical overflow system recommended for range -40...+80°C
    Stability ±0.05°C (at 20°C)
    Uniformity ±0.05°C
    Cooling gradient 0.4°C/min

  • Calibration liquid
    silicone oil 200C5

    Code: 200C5

    Can with 9 kg
    Silicone oil 200C5
    Application range -40...+130°C
    Smoke flash point at 110°C
    A viscosity of 10 cst
    exists at +5°C
    Freezing temperature -65°C

    To be used for devices with vertical overflow system for temperatures 0...+125°C.

  • Calibration liquid
    silicone oil 47V10

    Code: 47V10

    Can with 9 kg
    Silicone oil 47V10
    Application range -30...+150°C
    Smoke flash point at 150°C
    A viscosity of 10 cst
    exists at +20°C
    Freezing temperature -65°C

  • Calibration liquid
    silicone oil 47V20

    Code: 47V20

    Can with 9 kg
    Silicone oil 47V20
    Application range -20...+200°C
    Smoke flash point at 230°C
    A viscosity of 10 cst
    exists at +60°C
    Freezing temperature -60°C

    Recommended for devices without vertical overflow system for range -20...+125°C
    Stability ±0.05°C (at 20°C)
    Uniformity ±0.1°C
    Cooling gradient 1°C/min

  • LTC-AQ2SP2

    Aq2Sp2 Software

    Code: LTC-AQ2SP2

    Accessory:
    Windows®-PC software
    Control of the calibrator from the PC, manual or automatic calibration of one or more test items, load and endurance tests, thermostat tests (incl. hystersis), generation of calibration certificates

  • RS232-LTC-KABEL

    Special RS232 cable

    Code: RS232-LTC-KABEL

    Accessory:
    Special RS232 connection cable

  • RS232-USB-KONV

    RS232/USB converter

    Code: RS232-USB-KONV

    Accessory:
    Interface converter
    RS232 to USB

Information about operating fluids for temperature calibration baths

Calibration liquids for LR-Cal temperature calibration baths

Applications:

  • Thermostatic fluids for micro baths and thermostatic temperature calibration baths

Main Characteristics:

  • Operating range -50...+200°C
  • High stability
  • Good thermal conductivity
  • Nearly odourless
  • Long service live
  • Packaged in bottle or canister
  • Different types for a wide range applications
  • Low toxicity
  • Low viscosity and corrosovity

Our thermostatic fluids are suitable for use in liquid thermostatic calibrators and thermostatic baths for applications from -50°C to +200°C.
The choice of thermostatic fluid is the most important aspect for obtaining the best results with regard to operation and temperature control of calibrators and baths.
These fluids have perfect thermodynamic characteristics to guarantee the best performance in the various fields of application, ensuring safe and reliable operation as well as optimum heat transfer efficiency.
Silicone-based fluids are chemically inert substances that do not affect metals, are resistant to weathering and, when used correctly, the very low formation of cracking and oxidation ensures a long service life.

Most of our thermostatic fluids are available in different containers: 500 cm³ bottles or 9 kg canisters (25 kg on request).

Temperature application ranges of the various operating fluids:

Type of calibration
medium (liquid)
Usable
range
(1)
Temperature above which fume hood
should be provided
(2)
Fume
burning
(3)
A viscosity of 10 cst exists at a temperature of
(4)
Freezing temperature
(5)
Glycol 56% + water * -40...+90°C +70°C >110°C  +20°C -43°C
Silicone oil 47V5 -40...+130°C +110°C +136°C  +5°C  -65°C
Silicone oil 47V10 -30...+150°C +120°C +160°C  +20°C  -65°C
Silicone oil 47V20 -20...+200°C ** +130°C +230°C  +60°C  -60°C
Silicone oil 47V50 +30...+250°C ** +140°C +280°C  +160°C  -55°C
Silicone oil 47V100 +50...+200°C ** +170°C >300°C  +200°C  -55°C
Silicone oil 47V150 +50...+200°C ** +190°C >300°C  -/-  -55°C
Note: Note text:
* Mixture of 56% Glycol + 44% water
** In order to avoid gelling, it is recommended not to exceed a temperature of 200°C for a long time; even for fluids with wider operating ranges
(1) Usable range
The “usable range” of a calibration liquid is the temperature range in which it can be used under optimum conditions. The range may be limited by viscosity, flash points, freezing points, boiling points, evaporation rates, tendency to gel (or polymerize), etc.
There is no liquid that covers extremely wide temperature ranges. Therefore, you should ideally use a separate calibration liquid for each temperature range. The recommended range is the one in which the viscosity is not optimal, but still reaches values that allow proper use.
(2) Use of a fume hood
The use of an exhaust hood when using temperature calibration baths prevents users from inhaling vapors from calibration liquids. It is best to use extraction devices near the access opening to the calibration bath. Vapors can otherwise settle on the mucous membranes of the eyes or on the skin, causing discomfort. Silicone oils can form benzene and formaldehyde when they decompose at high temperatures. The table shows the temperature above which an extractor hood should be used.
(3) Flash point
The table shows the temperature value at which the presence of an open flame can ignite vapours combustion.
(4) Viscosity
Viscosity is a measure of the flow resistance of a liquid. Viscosity increases with decreasing temperature. Kinetic viscosity is the ratio of absolute viscosity to density. This is measured in stokes and centistokes (cSt). 1 cSt = 1 stoke divided by 100. The higher the cSt, the more viscous or dense the liquid. Excessively viscous liquids place a strain on the stirring and pumping mechanisms of the calibration bath and do not transfer heat sufficiently. The table shows the temperature value below which the performance of the temperature calibration bath is no longer optimal. The equivalent value of water at 20°C is 1.1 cst.
(5) Freezing point
Silicone oils also change their state below a certain temperature by solidifying. The table shows the value at which the calibration fluid changes its state and solidifies.

Other physical and chemical properties

Specific heat
The specific heat is the amount of heat required to raise or lower the temperature by 1 °C per kg. The specific heat, called CP, is expressed in Kcal/Kg °C. The energy required to heat or cool the calibration liquids depends on the amount of liquid contained in the calibrator in kg and its specific heat. A high specific heat value requires more energy to change the temperature, but offers greater temperature stability. The average CP of silicone fluids is 35 Kcal/Kg °C. The CP of water at 20 °C is equal to 1.

Thermal conductivity
Thermal conductivity is the ability of the liquid to transfer heat from one molecule to another. The better the heat transfer, the faster the liquid heats or cools. Better thermal conductivity improves the temperature uniformity in the reservoir of the calibration bath.

Expansion
All liquids have a coefficient of thermal expansion. This indicates how much the volume of a liquid changes (expands or contracts) when the temperature changes. Liquid expansion has an important impact on the safety, cleanliness and maintenance of temperature calibration baths. If calibrators are filled with too much liquid at a low temperature and then heated without regard to the increase in volume, they can overflow.

If too little liquid is filled in the reservoir, below the level of the heating elements, the temperature rise of the non-immersed part of the heating elements could ignite the liquid.

Gelation (polymerization)
The gelling temperature is the temperature at which silicone fluids oxidize, gel and turn into a viscous slurry. The main cause of this phenomenon is oxidation. Although silicone fluids can be used safely up to their flash point, the susceptibility to polymerization increases when used above their oxidation point. To prevent polymerization, it is advisable to keep the operating time above the oxidation point of the silicone oil used as short as possible in order to keep contaminants (salts, other oils and oxidizing agents) away. The calibration fluid must be replaced if it becomes dark, viscous or temperature unstable. It is important to limit the application time at high temperatures to prevent the oil from degrading and to extend its service life.

Read more …LR-Cal BK 40-M temperature calibration bath

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LR-Cal TB 300-M temperature calibration bath

LR-Cal TB 300-M
Stationary temperature calibration bath
+50...+300°C

LR-Cal TB 300-M stationary temperature calibration bath LR-Cal
  • Stationary
  • Temperature range +50°C...+300°C
  • Accuracy ±0.2°C, stability ±0.05°C
  • Calibration bath made of stainless steel, useful diameter 85 mm, depth 340 mm
  • Option: Version -2I with 2 measuring inputs for Pt 100 or thermocouples
  • Option: Vertical overflow system for even higher temperature uniformity
  • Control panel of the LR-Cal TB 300-M calibration bath

    Bedienpanel

    LR-Cal TB 300-M
    control panel

  • Vertical overflow system of the calibration bath LR-Cal TB 300-M

    Überströmsystem

    optional vertical
    overflow system

  • Schema Überströmsystem am LR-Cal TB 300-M

    Schema: Überströmsystem

    Scheme of the
    optional vertical
    overflow system

  • Description

    LR-Cal TB 300-M description

    The portable temperature calibration bath LR-Cal TB 300-M serves as a temperature source and reference instrument in one, for testing and calibrating temperature measuring instruments of all kinds. It is particularly suitable for laboratory and glass thermometers.

    It features a particularly robust design, with stainless steel liquid container, and modern microprocessor control.

    The large usable volume of approx. 10 liters ensures high temperature stability over the entire range, thus simultaneous calibration of several test items is possible without any problems. The vessel is filled with a suitable calibration medium, which is constantly kept in a homogeneous state by means of a vertical stirrer. The stirrer is driven by an 80W electric motor. The equipment is also equipped with a safety temperature limiter, an overflow and a valve for emptying the heating tank.

    Optionally, the LR-Cal TB 300-M temperature calibration bath can be equipped with a vertical overflow system to further improve temperature stability and uniformity.

    The thermostatic temperature calibration bath LR-Cal TB 300-M is used

    • Testing and calibration of temperature sensors
    • Testing and calibration of glass thermometers
    • Testing and calibration of measuring temperature chains
    • Testing and adjustment of thermostats and thermostatic valves

     

  • Variants/designs

    LR-Cal TB 300-M Variants/designs

    Code Variant / design
    TB300-M Normal standard version
    TB300-M-TR Variant with vertical overflow system for further improvement of temperature uniformity
    TB300-M-2I Version -2I with two measuring inputs for Pt 100 / thermocouples *)
    TB300-M-TR-2I Version with vertical overflow system and with two measuring inputs for Pt 100 / thermocouples *)

     

    *) Accuracy (maximum deviation) of the two measuring inputs for device version "-2I":
    Pt 100 or Pt 1000 at -40°C: ±0.09°C at 0°C: ±0.08°C at +150°C: ±0.11°C at +300°C: ±0.14°C
    Thermocouple type B at +950°C: ±0.97°C at +1050°C: ±1.03°C at +1,200°C: ±1.12°C    
    Thermocouple type E at -40°C: ±0.42°C at 0°C: ±0.40°C at +350°C: ±0.61°C    
    Thermocouple type J at +200°C: ±0.52°C at +450°C: ±0.67°C at +700°C: ±0.82°C    
    Thermocouples types K, N, R and S at +400°C: ±0.64°C at +700°C: ±0.82°C at +1,000°C: ±1.00°C    
    Thermocouple type T at -40°C: ±0.42°C at 0°C: ±0.40°C at +350°C: ±0.61°C    
  • Specification

    LR-Cal TB 300-M specification

    Description: Data:
    Temperature range +50°C...+300°C
    Stability ±0.05°C
    Uniformity 0.02°C radial and axial
    Stability indication audiovisual
    Accuracy ±0.2°C at +150°C
    Display resolution 0.01°C
    Temperature indication °C / °F switchable
    Interface RS232
    Thermostat test circuit 12V
    Ramp function yes
    Switch test yes
    Bath containter Stainless steel, usable diamter 85 mm, depth 340 mm
    Versorgung 230 VAC ±10% (optional, on request: 115 VAC)
    Leistungsaufnahme 2500 W
    Gewicht approx. 25 kg (Shipping weight approx. 35 kg)
    Abmessung 450 x 450 x 925 / 1300 mm
  • Scope of standard supply

    LR-Cal TB 300-M scope of standard supply

    • Stationary temperature calibration bath LR-Cal TB 300-M
    • Tank cover with 5 holes, 16 mm diameter, with guide tube
    • Spare fuses
    • Cable for power supply
    • Connection cables for thermostat tests
    • Holding device for test specimens
    • only for -2I versions: Connection cable red/black, screw terminals red/black, for both measuring inputs
    • Factory certificate of calibration
    • Operating manual EN
  • Calibration liquids + Accessories

LR-Cal TB 300-M calibration liquids + accessories

  • Calibration liquid
    Glycol

    Code: GLYCOL

    Can with 10 kg
    Ethylenic glycol 56%
    Application range -40...+80°C
    Smoke flash point at 110°C
    A viscosity of 10 cst
    exists at +20°C
    Freezing temperature -43°C

    For units with vertical overflow system to be used for temperatures -40...+1°C.

    For devices without vertical overflow system recommended for range -40...+80°C
    Stability ±0.05°C (at 20°C)
    Uniformity ±0.05°C
    Cooling gradient 0.4°C/min

  • Calibration liquid
    silicone oil 47V20

    Code: 47V20

    Can with 9 kg
    Silicone oil 47V20
    Application range -20...+200°C
    Smoke flash point at 230°C
    A viscosity of 10 cst
    exists at +60°C
    Freezing temperature -60°C

    Recommended for devices without vertical overflow system for range -20...+125°C
    Stability ±0.05°C (at 20°C)
    Uniformity ±0.1°C
    Cooling gradient 1°C/min

  • Calibration liquid
    silicone oil 47V100

    Code: 47V100

    Can with 9 kg
    Silicone oil 47V100
    Application range +50...+270°C
    Smoke flash point at 300°C
    A viscosity of 10 cst
    persists at +200°C
    Freezing temperature -55°C

    Stability ±0.05°C (at 200°C)
    Uniformity ±0,05°C
    Cooling gradient 6°/min

  • Calibration liquid
    silicone oil 47V710

    Code: 47V710

    Can with 9 kg
    Silicone oil 47V710
    Application range +80...+280°C
    Smoke flash point at 300°C
    A viscosity of 10 cst
    persists at +150°C
    Freezing temperature -22°C

    Stability ±0.05°C (at 200°C)
    Uniformity ±0,05°C
    Cooling gradient 6°/min

  • LTC-AQ2SP2

    Aq2Sp2 Software

    Code: LTC-AQ2SP2

    Accessory:
    Windows®-PC software
    Control of the calibrator from the PC, manual or automatic calibration of one or more test items, load and endurance tests, thermostat tests (incl. hystersis), generation of calibration certificates

  • RS232-LTC-KABEL

    Special RS232 cable

    Code: RS232-LTC-KABEL

    Accessory:
    Special RS232 connection cable

  • RS232-USB-KONV

    RS232/USB converter

    Code: RS232-USB-KONV

    Accessory:
    Interface converter
    RS232 to USB

Information about operating fluids for temperature calibration baths

Calibration liquids for LR-Cal temperature calibration baths

Applications:

  • Thermostatic fluids for micro baths and thermostatic temperature calibration baths

Main Characteristics:

  • Operating range -50...+200°C
  • High stability
  • Good thermal conductivity
  • Nearly odourless
  • Long service live
  • Packaged in bottle or canister
  • Different types for a wide range applications
  • Low toxicity
  • Low viscosity and corrosovity

Our thermostatic fluids are suitable for use in liquid thermostatic calibrators and thermostatic baths for applications from -50°C to +200°C.
The choice of thermostatic fluid is the most important aspect for obtaining the best results with regard to operation and temperature control of calibrators and baths.
These fluids have perfect thermodynamic characteristics to guarantee the best performance in the various fields of application, ensuring safe and reliable operation as well as optimum heat transfer efficiency.
Silicone-based fluids are chemically inert substances that do not affect metals, are resistant to weathering and, when used correctly, the very low formation of cracking and oxidation ensures a long service life.

Most of our thermostatic fluids are available in different containers: 500 cm³ bottles or 9 kg canisters (25 kg on request).

Temperature application ranges of the various operating fluids:

Type of calibration
medium (liquid)
Usable
range
(1)
Temperature above which fume hood
should be provided
(2)
Fume
burning
(3)
A viscosity of 10 cst exists at a temperature of
(4)
Freezing temperature
(5)
Glycol 56% + water * -40...+90°C +70°C >110°C  +20°C -43°C
Silicone oil 47V5 -40...+130°C +110°C +136°C  +5°C  -65°C
Silicone oil 47V10 -30...+150°C +120°C +160°C  +20°C  -65°C
Silicone oil 47V20 -20...+200°C ** +130°C +230°C  +60°C  -60°C
Silicone oil 47V50 +30...+250°C ** +140°C +280°C  +160°C  -55°C
Silicone oil 47V100 +50...+200°C ** +170°C >300°C  +200°C  -55°C
Silicone oil 47V150 +50...+200°C ** +190°C >300°C  -/-  -55°C
Note: Note text:
* Mixture of 56% Glycol + 44% water
** In order to avoid gelling, it is recommended not to exceed a temperature of 200°C for a long time; even for fluids with wider operating ranges
(1) Usable range
The “usable range” of a calibration liquid is the temperature range in which it can be used under optimum conditions. The range may be limited by viscosity, flash points, freezing points, boiling points, evaporation rates, tendency to gel (or polymerize), etc.
There is no liquid that covers extremely wide temperature ranges. Therefore, you should ideally use a separate calibration liquid for each temperature range. The recommended range is the one in which the viscosity is not optimal, but still reaches values that allow proper use.
(2) Use of a fume hood
The use of an exhaust hood when using temperature calibration baths prevents users from inhaling vapors from calibration liquids. It is best to use extraction devices near the access opening to the calibration bath. Vapors can otherwise settle on the mucous membranes of the eyes or on the skin, causing discomfort. Silicone oils can form benzene and formaldehyde when they decompose at high temperatures. The table shows the temperature above which an extractor hood should be used.
(3) Flash point
The table shows the temperature value at which the presence of an open flame can ignite vapours combustion.
(4) Viscosity
Viscosity is a measure of the flow resistance of a liquid. Viscosity increases with decreasing temperature. Kinetic viscosity is the ratio of absolute viscosity to density. This is measured in stokes and centistokes (cSt). 1 cSt = 1 stoke divided by 100. The higher the cSt, the more viscous or dense the liquid. Excessively viscous liquids place a strain on the stirring and pumping mechanisms of the calibration bath and do not transfer heat sufficiently. The table shows the temperature value below which the performance of the temperature calibration bath is no longer optimal. The equivalent value of water at 20°C is 1.1 cst.
(5) Freezing point
Silicone oils also change their state below a certain temperature by solidifying. The table shows the value at which the calibration fluid changes its state and solidifies.

Other physical and chemical properties

Specific heat
The specific heat is the amount of heat required to raise or lower the temperature by 1 °C per kg. The specific heat, called CP, is expressed in Kcal/Kg °C. The energy required to heat or cool the calibration liquids depends on the amount of liquid contained in the calibrator in kg and its specific heat. A high specific heat value requires more energy to change the temperature, but offers greater temperature stability. The average CP of silicone fluids is 35 Kcal/Kg °C. The CP of water at 20 °C is equal to 1.

Thermal conductivity
Thermal conductivity is the ability of the liquid to transfer heat from one molecule to another. The better the heat transfer, the faster the liquid heats or cools. Better thermal conductivity improves the temperature uniformity in the reservoir of the calibration bath.

Expansion
All liquids have a coefficient of thermal expansion. This indicates how much the volume of a liquid changes (expands or contracts) when the temperature changes. Liquid expansion has an important impact on the safety, cleanliness and maintenance of temperature calibration baths. If calibrators are filled with too much liquid at a low temperature and then heated without regard to the increase in volume, they can overflow.

If too little liquid is filled in the reservoir, below the level of the heating elements, the temperature rise of the non-immersed part of the heating elements could ignite the liquid.

Gelation (polymerization)
The gelling temperature is the temperature at which silicone fluids oxidize, gel and turn into a viscous slurry. The main cause of this phenomenon is oxidation. Although silicone fluids can be used safely up to their flash point, the susceptibility to polymerization increases when used above their oxidation point. To prevent polymerization, it is advisable to keep the operating time above the oxidation point of the silicone oil used as short as possible in order to keep contaminants (salts, other oils and oxidizing agents) away. The calibration fluid must be replaced if it becomes dark, viscous or temperature unstable. It is important to limit the application time at high temperatures to prevent the oil from degrading and to extend its service life.

Read more …LR-Cal TB 300-M temperature calibration bath

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